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-   -   Microcrystalline Wax (https://www.dvinfo.net/forum/alternative-imaging-methods/27433-microcrystalline-wax.html)

Obin Olson June 29th, 2004 07:34 PM

man Frank I don't care about what you shot I WANT TO SEE IT NOW!!!! LOL please? I really want to try this with our HD camera! do you think it's grainless enough for HD?

No, really can you tell me what type of wax you used I want to try it

Frank Ladner June 29th, 2004 09:43 PM

Obin: LOL! Ok, ok!

I uploaded three full size frames and one 352x240 video (DivX compressed AVI, about 1.12 MB).

The movie was shot handheld. I'm waving the camera around while holding the glass and lens to the front of the camera. So you may see some flare in there where I allowed light to come in.

The reason I chose this shot to show you guys was because I stopped down the 35mm lens and got no grain. It's harder to tell from the small resolution movie, so check out some of the framegrabs.



http://www.frankladner.com/m_001.jpg
http://www.frankladner.com/m_002.jpg
http://www.frankladner.com/m_003.jpg

http://www.frankladner.com/micro_test_01.avi

(Note: m_002.jpg is motion blurred a bit, not diffused/softened by the glass.)

Again, this is using a layer of microcrystalline wax between two pieces of glass (small, cheap picture frames). I stick two aluminum foil strips (folded a couple of times) inbetween the glass on the sides. I then tape the sandwich around the top and bottom and set it vertically in the melted wax. (Read previous posts for more details.)

To you guys that may try this, it's pretty simple to do, but the biggest problem is getting all those little air bubbles out, even when the glass sandwich is vertical.

I had good results with taping the sides and bottom, so that no wax could leak out, and spooning melted wax over the top, filling the glass up. Then I'd let it sit for a while so most of the air bubbles would get out. This gave me one usable side of the glass.
(btw, the picture frames are rectangular. I'm looking for some small, cheap square ones. Maybe I'd have less trouble w/ air bubbles if I was using smaller pieces of glass.)

I am still trying for the (almost) perfect glass. Once I get that, I'll build some sort of housing and try to make it look good (and more importantly, keep the light out).

Any more suggestions would be really appreciated.

,Frank

Obin Olson June 29th, 2004 10:06 PM

wow lookin good!! can you please upload some stills that are Not stopped down so i can see some details? give me a still from the first sec of the video that is wide open..what camera are you using?

Frank can you make me one for testing with my HD camera and see if i can see grain with HD?

Rai Orz June 30th, 2004 05:18 AM

Frank, it makes me happy to see the good results in so short time. As i said before, we worked since years with 35mm solutions and the wax way is still the best. Our GG was developed together with a manufacturer for fine optical parts. We tested hundreds ways with hundreds different mixtures. The way i told before in this thread (its nearly the way you make it) brings the best. But it is not grainless. The grain is surely very smal, but a HD Cam with more than 720 vertical lines (and exact focos!!!) can see it. That is the reason why we bring the GG also in very smal and loudless, circle vibrations. This requires a very exactly fine-mechanical work. We found pvc was not well enoug, so our System is make in aluminum. Also we tested everyone on a optical bank. This time we work on a little different way for a cinema solution with a HD Cam with more than 2000 vertical lines. Because The patent examinations is going on, i can not yet say more details. Please wait another few days.

Obin Olson June 30th, 2004 06:58 AM

Rai, will 1280x720 see the grain?

Frank Ladner June 30th, 2004 08:16 AM

Rai: Thanks! A high-def. with the ability to use 35mm lenses is the ultimate camera solution, I think. Especially if you can use variable framerates.

Obin: Thanks! I will try to post some 720x480 framegrabs from the first part of the movie when I get home. Oh, and I am using a Canon GL2.

Rai Orz June 30th, 2004 08:18 AM

Obin, 720 verical lines is the border between visible and invisibly if you use a sill picture lens. I think your camera supply 1024 lines, but you would like to use only 720 so with the width of 1280Pixels you have a 16:9 format. If this is so, the picture on the GG is round 37,6 x 21,2mmm. This means, with 720lines, you have 33,9lines/mm. If you use a 4:3 format, your picture can be up to 34,5 x 25,8 and with 720lines, you have only 27,9lines/mm. But if you wont to use a original movie frame size, with only 16mm high, you have 45lines/mm.
So, if you use the 16:9 format with 21,2mm hight, the grid will be visible. Maybe we test next time also the SI-1300RGB, and maybe we create a 35mm solution (with our new GG) particularly for this cam together with a nice classical rounded "moviecam-like-housing" for the whole unit.

Obin Olson June 30th, 2004 08:50 AM

Yes I will be designing a "movie-cam-like-housing" very soon ;)
so at 16x9 1280x720 you think that I will see the gg grain from wax?

Rai Orz June 30th, 2004 12:32 PM

Obin, the "normal" wax technologie is what bosscreen use. You know the problems with bossscreen or intenscreen or so on. Microcrystalline wax has a fine grid, but the main different here is the very small space. But it is only the half way. Try it out. 1280x720 on a 37,6 x 21,2mmm frame size and you will see the gg grain.
Obin, lets work together, my company make not toys. And we not only have a HD 35mm solution, we have for example a low cost Follow Focus System for every still photo lens, with or without servo motors (And you need that with a 35mm DOF).
We also like to create a low cost HD CAM with 35mm DOF and other movie features. Today, we have contacted siliconimaging. Lets see...

Jesse Rosten June 30th, 2004 12:36 PM

Rai -

In your previous post you said to use 90% paraffin wax and 10% bee's wax. Is this better than using 100% microcrystalline wax? What's the difference between paraffin and microcrystalline wax?

This thread is exciting. Can't wait to see more pics, Frank.

Rai Orz June 30th, 2004 01:03 PM

Jesse, what is microcrystalline wax? I think a product name of Strahl & Pitsch. I canīt say what mixture it is. I know it is natural wax and we also tested it years ago. We dont had a way to change the mixture, so we make more tests with basic products like paraffin and bee's wax. We also make tests with chemical products.

Frank Ladner June 30th, 2004 01:38 PM

Jesse: Microcrystalline wax is characterized by its small grain.

Check these links out:

http://www.britannica.com/eb/article...paraffin%20wax

http://www.calwax.com/products/Microcrys.asp

Rai Orz July 1st, 2004 03:04 AM

Frank, thanks. We will check it soon, but the man who made our tests with microcrystalline wax is in vacation. So i canīt say details yet. The only thing i can say, with the other method our results are better.

Bob Hart July 10th, 2004 05:30 AM

Rai.

I made a wax brew of 90%/10% and applied it between two oharadisks (glass CDs). Through a magnifier, the grain structure is about the same as the normal ground-glass dressed with 5 micron aluminium oxide powder water slurry.

The size grading of this grain structure varies across the disk which brings back the problem of variable density flicker I had with the plastic CD-R disks. This is why I went to optical glass.

Is there a subsequent annealing process to make the grain structure even across the screen?

Images through the rotating "boss screen" do not seem to be sharper but the colour seems brighter.

Bob Hart July 11th, 2004 01:01 AM

Furthur to above, there are some images posted at "www.dvinfo.net/media/hart" titled "waxds002.jpg" or similar which are a test of a rotary wax composite disk. You'll have to put the address in by hand as it is not a link. I've forgotten how to do that href thing to embed addresses in the text.

Matthew Miller July 11th, 2004 02:20 AM

Do any of you guys with the microcrystalline wax have like a 3 megapixel camera? Couldn't you use that instead of a DV camera to determine at what resolutions the grain becomes visible?

I have an 8 megapixel camera, and a Nikon Lens. Right now, I'm just starting to experiment with all the stuff I've been reading here. My first GG was just a piece of a white plastic bag stretched tight as a drum. Then I graduated to the school of rotating GGs and took a beltsander to a CD-R.

So I guess I should get my hands on this wax mix and start taking some hi-res comparison pictures of the different GG methods.

Obin,
I'm pursuing getting my hands on a nice wide angle Medium Format lens, just in case a 1280x720 sensor ends up seeing the grain too much when focusing on a square the size of 35mm film. The image projected onto the GG from a Medium Format lens should be over twice the size of what the 35m lens projects. And I've been reading all I can about depth of field to figure out if the medium format will be too different from a 35mm lens to get the 'movie' look we're all going for here.

Bob Hart July 11th, 2004 09:34 AM

Matthew.

Although my tests with wax were shot with a rotating disk, I can advise that the grain structure was of a size similar to the AO 5 micron dressed optical glass disk.

I had no access to 3 micron so I allowed the 5 micron to wear down to exhaustion for a finer finish and partial polish-back. A polish-back seemed to confer a better clarity and brightness with plastic CD-R spacers.

With the glass, this is a bit tricky. If you leave the slurry in that state for too long, the glass hangs on the dressing sheet and gets gouges in it.

When shooting with the glass and CD-R, the spinning disk eliminated the grain as such but another effect in strong backlight, I describe as scintillation similar to snow or video noise, but of a finer texture, becomes apparent. It was subjectively like fine film grain.

It was more so with the glass disk until I went to the 5 micron and degraded the image even with the spinning disk. I theorise that the form of the abrasions in the glass and CD-R creates random pinpoint flashes of light under these conditions. It may be visible in the still image mtatk2f2.jpg in the background behind the guitar player. It was on the DVD.

You can see this effect in some of the still images even though the disk was moving. If some of the frame captures are enlarged heavily, you can see a pattern of blockiness of about 8 pixels area, where the DV codec is struggling with the high rate of subtle change between frames.

The wax disk originations dont seem to do this. Instead you see a pattern of slightly darker or lighter patches in the image more like very faded freckles. My theory for what it is worth is that whilst the wax disk that I have made does not yield a finer resolution, it does not introduce so much fine textured highlight variation in the image from frame to frame, so the codec does not have to play an aggressive averaging game with the resolution, therefore the image appears to be clearer. This is not of much help for fixed groundglasses. I think that whilst the grain structure is there i9n wax, it does not seem as sharply facetted like the glass texture is.

The beeswax portion of your brew will have to be carefully cared for as it darkens with overheating. It melts lower than boiling point of water and slightly before the paraffin and seems to have a tendency to settle out. Hold your glass above the brew in the heat for a while to preheat it before you drown it so you don't crack it. Likewise, don't haul it out into cold air in any haste.

Martin Lindstedt July 24th, 2004 11:39 AM

the bubbles!!
 
I recieved my microwax about a week ago, and I've been trying different ways to minimize the airbubbles the last few days, however with no obvious success.

I've tried bonding the glasses at the sides and bottom, and then submerge it into the wax. What I can't figure out is why some airbubbles insist on staying between the glass. Even though I let the glasses sit in the hot wax for a while ( hell, I let it sit for two hours!! ). Any ideas anyone, to get those bubbles out??

One thing I discovered while experimenting, when I accedentaly dropped some hot wax into my pot with boiling water. When I was done for the day, and let the pot cool off, the wax solidified pretty evenly, on top of the water. The layer was too thick though, but if you poured just a small amount of wax into the boiling water, perhaps it could be carefully taken out once solidified?

Bob Hart July 24th, 2004 09:41 PM

If there is a slight imperfection in the glass surface or a minute speck of dust, an air bubble will hang instead of moving up.

When making my composite disks, I found I had to place one disk in the melted wax, then lower the other disk into the brew at an angle so it became wetted and any bubbles moved off, then lower it on to the lower disk.

Because I kept the temp low, I was able to use a CD-R spindle to preserve alignment but getting the disks off it afterward was a problem.

I used pieces of cooking foil for spacers between the disks. TO prefvent them from moving, I glued them to the glass with PVC wood glue (I think you folk call it Elmers) on the outside surface and folded them under to provide the spacer. The glue washes off afterwards and the spare foil is trimmmed off.

Due to the method I used to figure and polish the disks, there was too much surface variation for them to be used back to back with any hope of a consistent thickness of wax between them.

I found this to be the cause of the variable density flicker I have previously described.

To melt the wax I have used an electic cookpot which has a sensor control somewhat like an electric frypan and will hold good temp control at or below water boiling point.

To clean your wax off the outside of the glass, use a fine razor or scraper blade, then use Preen trigger spray, then water and kitchen detergent, then methylated spirit or blue window cleaner.

Justin Burris July 25th, 2004 12:39 AM

Just a thought here: when you get a chip in your windshield, and they come out to patch it, I understand that they put some sort of gel on the outside of the windshield where the chip is, then use suction on the inside which instantaneously sucks the gel into every little crevice. From what I have heard, once they have done this, you can't tell there was ever a chip.

I have to imagine this has potential for us. If we were to begin to submerge the two pieces of glass into the wax, then somehow apply suction at the top, thereby forcefully drawing the molten wax into the sliver of space between them...
I don't have any wax yet, so I am unable to try it, but Martin, if you are game, maybe this will be the ticket. Got a vacuum cleaner?

Martin Lindstedt July 25th, 2004 04:45 AM

haha! .. vacuum cleaner! :)

I actually had this idea a while ago .. sucking up the wax .. but the problem would be to keep the wax inside when you remove it from the pot .. hmm .. but it's worth a shot, though !

Bob, are you saying that wax isn't good enough to be used as a GG? Have you tried microwax after your paraffin and beeswax mix?

Another technique is to make a frame of aluminium foil on a glass, the pour hot wax in the middle, and then smash another glass on top of it, forcing any bubbles out. But I guess the wax is too .. "waterish" to make this work.

Anyone knows what technique they use to make those Bosscreens?

Bob Hart July 25th, 2004 05:32 AM

Using a vacuum is legitimate provided you preheat your glass to keep the wax liquified. Maintain the vacuum and wax supply whilst you cool the glass. Any entrained air in the wax will expand furthur under a vacuum. (There may be a problem with light fractions vaporising in vacuum conditions and making furthur bubbles or density inconsistencies in the mix but this one is theoretical).

I have only used the 10% beeswax blend. The waxdisk.jpg files on www.dvinfo.net/media/hart were doens with this brew.

I have not yet found a handy source of micro-crystalline wax in W.A.. We do have a petrol refinery nearby so it might turn up there.

The aluminium foil idea is a dead-end or at least in the method I used. It is too hard to immobilise unless you fold tags over to glue it on back of the glass. It tends to expand, float and crinkle which spoils the precision between the glass panels.

I tried centrifugal force by spinning the disks and the CD-R spindle under the wax to make the bubbles migrate to the center however sooner or later you have to stop in order to haul the composite disk out and any bubbles go back to the widest points between the two surfaces.

I think the best method will be to bring the two glasses together under the surface whilst holding them in a vertical position, then slowly laying them over, cooling the mix until at butter consistency then hauling the composite out to set hard. This requires more wax than I have on hand at the moment and a taller hotpot than I possess right now.

Frank Ladner July 25th, 2004 04:36 PM

I found out the hard way that even a fingerprint on the inside of the glass will trap tiny air bubbles inside. The inside layers have to be super clean.

Also, instead of heating a bunch of wax in a pot to get a enough for me to submerge the glass in, I just formed an aluminum cup (make sure to double layer it, though, depending on the foil's strength) and poured the hot wax in there. Then I submerged the glass sandwich (which consisted of two .99 cent picture frames, about 50mm in diameter, with a couple of folded bits of aluminum foil in between them and JB Weld around the sides, except for a notch at the top.) This would fill with wax and the air bubbles would rise to the top and out the opening. It needs to sit for a while, because those air bubbles are slow moving. I have found that it helps to take a pair of tongs and squeeze the glass a little, forcing the bubbles to work their way up more quickly.

For cleaning the outside of the glass after the wax had cooled, I would use a hair dryer - and just enough to heat the outside wax. Then I'd just clean it off with a rag.

Hope this helps!

,Frank

Bob Hart July 25th, 2004 10:16 PM

Hair dryer - now I wish I had thought of that.

Frank Ladner July 26th, 2004 01:14 PM

:-)

But you have to be careful and use the hairdryer on a low power, otherwise you might make a mess.

Or you can apply some paper directly over the wax and heat that. Most of the melted wax will soak into the paper. The rest you can just clean with a rag.

Filip Kovcin July 27th, 2004 05:01 PM

is this weird?
 
did anyone of you tryed to make proper GG with silicone glue? (not colored, but semi transparent one)
i mean to put super thin layer on glass - and when silicone is dry it's almost proper transparency for GG - or not?

what do you think?

filip

Frank Ladner July 27th, 2004 08:03 PM

Here's a 10 frame JPG sequence for you guys to check out.

It is slightly out of focus, which is one of the best ways to get grain to show up.

No post has been done except for the letterboxing.

http://www.frankladner.com/images/tree_pan_00000.jpg
http://www.frankladner.com/images/tree_pan_00001.jpg
http://www.frankladner.com/images/tree_pan_00002.jpg
http://www.frankladner.com/images/tree_pan_00003.jpg
http://www.frankladner.com/images/tree_pan_00004.jpg
http://www.frankladner.com/images/tree_pan_00005.jpg
http://www.frankladner.com/images/tree_pan_00006.jpg
http://www.frankladner.com/images/tree_pan_00007.jpg
http://www.frankladner.com/images/tree_pan_00008.jpg
http://www.frankladner.com/images/tree_pan_00009.jpg

Let me know what you guys think.

Thank you!

Les Dit July 27th, 2004 08:23 PM

Looks pretty good Frank. I only see a tiny amout of fixed pattern grain.
-Les

<<<-- Originally posted by Frank Ladner : Here's a 10 frame JPG sequence for you guys to check out.

It is slightly out of focus, which is one of the best ways to get grain to show up.

Let me know what you guys think.

Thank you! -->>>

Frank Ladner July 28th, 2004 09:31 AM

Les: Thanks for checking them out!

I've noticed that I don't have as bad of a hotspot with wax as opposed to ground glass. I believe this is due to the thickness of the wax layer, so if you had a thinner layer, you'd get a brighter image w/ hotspot similar to glass.

With a rotating device, however, I feel that it would be better/safer to use regular ground glass (in conjunction with condensers to remove hotspot) so that you wouldn't have to worry about the wax eventually melting or changing color.

Justin Burris July 28th, 2004 12:14 PM

Frank,

Image sequence looks great.

How thick is the wax?

Frank Ladner July 28th, 2004 12:40 PM

Justin: Thanks!

Well...I can't say an exact measurement of the wax thickness but this should give you an idea: I took a couple of thin strips of aluminum foil (regular stuff - not heavy duty) and folded them a couple of times to make the spacers between the two pieces of glass.

I'd say the thickness is a bit less than that of your fingernail.

Justin Burris July 28th, 2004 03:27 PM

Frank,

Would it be asking too much for another slow-pan image sequence, this one being a little longer (20?), and having something - that tree would work fine - in focus?

I only ask because this method that you are developing appears, at this point, to be our best bet for a static adaptor.

Thanks.

Frank Ladner July 28th, 2004 07:50 PM

Justin: Sure! I just sortof ran outside and grabbed that blurry tree footage just for the pan test. I'll get some in-focus shots tomorrow (It's dark right now.) and hopefully have a longer sequence uploaded.

Frank Ladner July 29th, 2004 04:25 PM

New Sequence
 
I uploaded 30 jpg frames from a sequence captured today.

Sorry these aren't zipped. (Don't have a zip program at the moment.)

http://www.frankladner.com/images/micro_00000.jpg

through

http://www.frankladner.com/images/micro_00029.jpg


Just copy/paste and change the number. Again, sorry about these not being zipped!

Thanks!

Filip Kovcin July 29th, 2004 04:37 PM

Re: New Sequence
 
<<<-- Originally posted by Frank Ladner : I uploaded 30 jpg frames from a sequence captured today.... -->>>

frank, the last jpg i downloaded was with nr 18, after that - i just see info - 'page not found'. i beleive that something is wrong with your page(s).

please - recheck your site. thank you.

filip

Frank Ladner July 29th, 2004 04:42 PM

Filip: Sorry about that! It's because the images weren't there yet. I had them uploading (on dialup) as I was posting the message.

:-)

Frank Ladner July 30th, 2004 10:16 AM

Going back and looking at those images...I still didn't have it in exact focus. (Hard to do with a small viewfinder.)

Les Dit July 30th, 2004 11:54 AM

Maybe you can 'rack focus' while it's recording. That way, we can see the DOF and something will be in focus.
-Les

Frank Ladner July 30th, 2004 12:00 PM

Les: Thanks for the suggestion! I'll try to get some new footage uploaded in the next couple of days.


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